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Résidus de pesticides dans le miel

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FOODS 24/09/21 Occurrence of Pesticide Residues in Spanish Honey Measured by QuEChERS Method Followed by Liquid and Gas Chromatography–Tandem Mass Spectrometry. In the current study, the QuEChERS extraction method with slight modifications, followed by liquid and gas chromatography–tandem mass spectrometry, was applied for the determination of 399 pesticide residues in 91 raw honey samples from northeastern Spain.

FOODS 24/09/21 Occurrence of Pesticide Residues in Spanish Honey Measured by QuEChERS Method Followed by Liquid and Gas Chromatography–Tandem Mass Spectrometry

The quality control procedure established in Document No. SANTE/12682/2019 was successfully followed: the responses in reagent blank and blank honey samples were below 30% of the reporting limit (0.01 mg kg−1) for all analysed compounds, the correlation coefficients (R2) were higher than 0.99 in most calibration curves, the deviation of back-calculated concentration from the true concentration was below ±20% (using the standard of 50 μg L−1 concentration), and the recoveries of spiked samples on matrix were within the range of 70–120% for almost all analytes. Only chlorfenvinphos (2–7.8 ng/g) and coumaphos (8.8–37 ng/g) were detected in 13 samples, and neither were observed to exceed their maximum residue limits (MRLs).

ENVIRONMENTS 03/07/21 Agrochemical Contamination of Honey and Bee Bread Collected in the Piedmont Region, Italy. All articles published by MDPI are made immediately available worldwide under an open access license.

ENVIRONMENTS 03/07/21 Agrochemical Contamination of Honey and Bee Bread Collected in the Piedmont Region, Italy

No special permission is required to reuse all or part of the article published by MDPI, including figures and tables. For articles published under an open access Creative Common CC BY license, any part of the article may be reused without permission provided that the original article is clearly cited. Feature Papers represent the most advanced research with significant potential for high impact in the field.

Feature Papers are submitted upon individual invitation or recommendation by the scientific editors and undergo peer review prior to publication. The Feature Paper can be either an original research article, a substantial novel research study that often involves several techniques or approaches, or a comprehensive review paper with concise and precise updates on the latest progress in the field that systematically reviews the most exciting advances in scientific literature. Scientific Papers of the University of Pardubice - 2020 - Determination of selected pesticides in honey and mead by HPLC.

ENVIRONMENTAL ENTOMOLOGY 03/12/18 Comparison of Pesticide Exposure in Honey Bees (Hymenoptera: Apidae) and Bumble Bees (Hymenoptera: Apidae): Implications for Risk Assessments. Skip to Main Content Sign In Register Close Advanced Search.

ENVIRONMENTAL ENTOMOLOGY 03/12/18 Comparison of Pesticide Exposure in Honey Bees (Hymenoptera: Apidae) and Bumble Bees (Hymenoptera: Apidae): Implications for Risk Assessments

Nicotinoïdes et miel. NATURE 19/04/17 High pesticide risk to honey bees despite low focal crop pollen collection during pollination of a mass blooming crop. Field experimental design In April 2015, we purchased 120 5-frame nucleus colonies of honey bees from a local commercial beekeeper.

NATURE 19/04/17 High pesticide risk to honey bees despite low focal crop pollen collection during pollination of a mass blooming crop

All nucleus colonies were transferred into new 10-frame equipment with plastic foundation and allowed to draw comb for two weeks in a common location (Dyce Lab for Honey Bee Studies, Ithaca, NY: 42.466118, –76.446211). During this time, all colonies were assessed for strength and queen status. Of the 120 colonies, 5 were determined to be queenless and replaced with new queens from the same genetic source. Following assessments, frames were redistributed among colonies such that all colonies had a similar composition of brood, bees, pollen and nectar prior to enrollment in the field experiment. NATURE 05/10/17 Controversial pesticides found in honey samples from six continents. Journal of Environmental and Public Health Volume 2017 (2017), Pesticide Residues in Honey from the Major Honey Producing Forest Belts in Ghana.

ROTHAMSTED RESEARCH 06/10/17 VIEWPOINT: NEONICOTINOID PESTICIDES IN HONEY. ENVA - 2016 - Thèse en ligne : Les résidus de médicaments vétérinaires et de pesticides dans les produits alimentaires apicoles (miel, pollen, gelée royale et propolis) ANSES/MAAF – JANV 2017 - Bulletin épidémiologique Santé animale - alimentation. Au sommaire: Numéro spécial surveillance sanitaire des aliments. Résultats des plans de surveillance et de contrôle des résidus de pesticides dans le miel en 2014 et 2015.

BERLIN_DE 28/06/16 Hundertfache Glyphosat-Menge in Honigprobe aus Brandenburg. Journal of Chromatography A Volume 1427, 4 January 2016, Pages 142–160 Simultaneous determination of 200 pesticide residues in honey using gas chromatography–tandem mass spectrometry in conjunction with streamlined quantification approach. A Central Laboratory of Residue Analysis of Pesticides and Heavy Metals in Food, Agricultural Research Center, Ministry of Agriculture and Land Reclamation, Giza, Egyptb Analytical Chemistry Department, Faculty of Pharmacy, Cairo University, Cairo, Egyptc Bioanalysis Research Group, Faculty of Pharmacy, Cairo University, Cairo, Egyptd Pharmaceutical Chemistry Department, Faculty of Pharmaceutical Sciences and Pharmaceutical Industries, Future University, Cairo, Egypt Received 2 October 2015, Revised 6 November 2015, Accepted 22 November 2015, Available online 2 December 2015 Choose an option to locate/access this article: Check if you have access through your login credentials or your institution Check access Get rights and content Highlights Modified QuEChERS protocol coupled to GC–MS/MS was developed and validated.

Journal of Chromatography A Volume 1427, 4 January 2016, Pages 142–160 Simultaneous determination of 200 pesticide residues in honey using gas chromatography–tandem mass spectrometry in conjunction with streamlined quantification approach

INSECTS 01/03/16 Effects of Pesticide Treatments on Nutrient Levels in Worker Honey Bees (Apis mellifera) Academic Editor: Brian T.

INSECTS 01/03/16 Effects of Pesticide Treatments on Nutrient Levels in Worker Honey Bees (Apis mellifera)

Forschler Received: 21 November 2015 / Revised: 10 February 2016 / Accepted: 22 February 2016 / Published: 1 March 2016 Honey bee colony loss continues to be an issue and no factor has been singled out as to the cause. In this study, we sought to determine whether two beekeeper-applied pesticide products, tau-fluvalinate and Fumagilin-B®, and one agrochemical, chlorothalonil, impact the nutrient levels in honey bee workers in a natural colony environment. Treatments were performed in-hive and at three different periods (fall, spring, and summer) over the course of one year. This is an open access article distributed under the Creative Commons Attribution License (CC BY 4.0).

Never miss any articles matching your research from any publisher Get alerts for new papers matching your research Find out the new papers from selected authors Updated daily for 49'000+ journals and 6000+ publishers Define your Scifeed now MDPI and ACS Style. Bulgarian Journal of Agricultural Science, 21 (Supplement 1) 2015, 208–212 THE PRESENCE OF LINDANE IN DIFFERENT TYPES OF HONEY IN THE PANNONIAN REGION. CATAGLYPHIS 03/01/16 Le miel et les pesticides (réponse de Alain Lenoir - professeur émérite - Université François Rabelais TOURS) Bulgarian Journal of Agricultural Science, 21 (Supplement 1) 2015, 208–212 THE PRESENCE OF LINDANE IN DIFFERENT TYPES OF HONEY IN THE PANNONIAN REGION.

Chemosphere Volume 120, February 2015, Residues of organochlorine and synthetic pyrethroid pesticides in honey, an indicator of ambient environment, a pilot study. Pesticides et santé des abeilles. JO ASSEMBLEE NATIONALE 25/08/15 Réponse à question: QE 86108 produits dangereux - pesticides - utilisation. conséquences. apiculture. Texte de la question Mme Marie-Françoise Clergeau appelle l'attention de M. le ministre de l'agriculture, de l'agroalimentaire et de la forêt, porte-parole du Gouvernement sur la situation de la filière apicole.

JO ASSEMBLEE NATIONALE 25/08/15 Réponse à question: QE 86108 produits dangereux - pesticides - utilisation. conséquences. apiculture

Selon une enquête rendue publique en mars 2015 par la Commission européenne, cette filière serait particulièrement menacée. Plusieurs facteurs jouent un rôle dans la hausse continue de la mortalité des colonies d'abeilles qu'il s'agisse du développement de prédateurs invasifs comme le frelon asiatique, de facteurs pathogènes nouveaux mais surtout et principalement des effets des insecticides utilisés dans le domaine agricole intensif. 30 % des ruches périssent chaque année en France. L'effondrement des colonies peut atteindre jusqu'à 80 % dans certaines régions entraînant une baisse considérable de la production dans notre pays de 32 000 tonnes en 1995 à 10 000 tonnes en 2014.

UNIVERSITE DE LIEGE - 2005 - Development of a quantification method for up to 50 pesticides in honey and beeswax by LC-MS/MS and GC-MS detection. J Environ Sci Health B. 2006;41(2):159-65. Determination of acaricide residues in saudi arabian honey and beeswax using solid phase extraction and gas chromatography. J Agric Food Chem. 2015 May 13;63(18):4484-92. QuEChERS Adaptability for the Analysis of Pesticide Residues in Beehive Products Seeking the Development of an Agroecosystem Sustainability Monitor. AGROSCOPE - MARS 2003 - Pesticide residues in honey and Beeswax produced in Switzerland. Acta Sci., Anim. Sci. vol.34 no.4 Maringá Oct./Dec. 2012 Pesticides in the propolis at São Saulo State, Brazil.

Pesticides in the propolis at São Saulo State, Brazil Pesticidas na própolis do Estado de São Paulo, Brasil Ricardo de Oliveira OrsiI, *; Lidia Maria Ruv Carelli BarretoII; Silvia Maria Alves GomesI; Samir Moura KadriI IDepartamento de Produção e Exploração Animal, Faculdade de Medicina Veterinária e Zootecnia de Botucatu, Universidade Estadual Paulista "Júlio de Mesquita Filho", Distrito de Rubião Júnior, s/n, 18618-000, Botucatu, São Paulo, Brazil IIDepartamento de Agronomia, Universidade de Taubaté, Taubaté, São Paulo, Brazil The increasing demand for propolis has caused a raise in its production.

Acta Sci., Anim. Sci. vol.34 no.4 Maringá Oct./Dec. 2012 Pesticides in the propolis at São Saulo State, Brazil

However, an increasingly pesticide-dependent agriculture is a great concern with regard to bees, their produce and environmental contamination. Keywords: environmental, Apis mellifera, agrochemicals, contamination. A crescente procura pela própolis tem ocasionado aumento em sua produção. JOURNAL OF ENVIRONMENTAL STUDIES - 2014 - Determining Pesticide Residues in Honey and their Potential Risk to Consumers. J Bioproces Biotech 2014, 4:7 Determination of Pesticide Residues in Honey using the GC×GC-TOFMS Technique. ITALIAN JOURNAL OF FOOD SAFETY – MAI 2014 - Rapid modified QuEChERS method for pesticides detection in honey by high-performance liquid chromatography UV-visible. Abstract The extensive use of pesticides in agriculture plays an important role in bees die-off and allows the presence of residues in hive products, particularly in honey.

ITALIAN JOURNAL OF FOOD SAFETY – MAI 2014 - Rapid modified QuEChERS method for pesticides detection in honey by high-performance liquid chromatography UV-visible.

An accurate and reliable analytical method, based on QuEChERS extractive technique, has been developed for the quantitative determination by high-performance liquid chromatography UV-visible detector of 5 pesticides (Deltamethrin, Dimethoate, Imidacloprid, Acetamiprid, Chlorfenvinphos) in honey. The method, according to Commission Directive 2002/63/EC and Regulation 882/2004/EC, provided excellent results with respect to linearity (correlation coefficient up to 0.993), limits of detection and quantification (0.005 and 0.01 μg/mL for Dimethoate, Deltamethrin and Chlorfenvinphos; 0.02 and 0.05 μg/mL for Acetamiprid and Imidacloprid), recovery values (86.4 to 96.3%), precision and relative expanded uncertainty of a measurement, demonstrating the conformity of the this method with the European directives.

Keywords. HARVARD GAZETTE - JUILLET 2015 - Pesticide found in 70 percent of Massachusetts’ honey samples. More than 70 percent of pollen and honey samples collected from foraging bees in Massachusetts contain at least one neonicotinoid, a class of pesticide that has been implicated in Colony Collapse Disorder (CCD), in which adult bees abandon their hives during winter, according to a new study from Harvard T.H.

HARVARD GAZETTE - JUILLET 2015 - Pesticide found in 70 percent of Massachusetts’ honey samples

Chan School of Public Health. The study appeared online in the July 23 issue of the Journal of Environmental Chemistry. JO ASSEMBLEE NATIONALE 20/01/15 Au sommaire: QE 72186 produits dangereux - pesticides - utilisation. conséquences. apiculture. Texte de la question M. Lucien Degauchy interroge M. le ministre de l'agriculture, de l'agroalimentaire et de la forêt, porte-parole du Gouvernement sur l'utilisation des traitements de semences à base de néonicotinoïdes, utilisés en culture de betteraves sucrières sous la forme d'un enrobage des semences. Les données recensées jusqu'ici ne donnent aucune indication tendant à démontrer que ces interdictions améliorent la santé des abeilles.

Dans le cas des semences de betteraves à sucre, il semble que la dissémination des poussières de semences ne constitue pas un risque pour les abeilles. De plus une interdiction de ces traitements pourrait réduire jusqu'à 20 % la production de betteraves sucrières. Texte de la réponse Concernant les produits phytopharmaceutiques, la Commission européenne a adopté en mai 2013, avec le soutien actif de la France, le règlement (UE) 485/2013 qui comprend des dispositions concernant trois néonicotinoïdes (clothianidine, imidaclopride et thiaméthoxam). J. Braz. Chem. Soc. vol.25 no.8 São Paulo Aug. 2014 Multiresidue determination of pesticide residues in honey by modified QuEChERS method and gas chromatography with electron capture detection.

Multiresidue determination of pesticide residues in honey by modified QuEChERS method and gas chromatography with electron capture detection Débora Orso; Manoel L. Martins; Filipe F. Donato; Tiele M. Rizzetti; Magali Kemmerich; Martha B. Adaime; Renato Zanella* J. Braz. Chem. Soc. vol.25 no.8 São Paulo Aug. 2014 Multiresidue determination of pesticide residues in honey by modified QuEChERS method and gas chromatography with electron capture detection.

Dalhousie University 16/12/13 Pesticides in Honey Bee Hives in the Maritime Provinces: residue levels and interactions with Varr. Extension Apiculturist, UC Davis - OCT 2013 - Honey Bees and Pesticides. UNIVERSITE D AVIGNON - 2012 - thèse en ligne : Effects of pesticides on honey bees (Apis mellifera L.): study of a specific rout. Journal of Food Research; Vol. 3, No. 2; 2014 Risk Assessment of Heavy Metals and Pesticides in Honey From Sicily (Italy) PLOS 15/10/13 Using a Hazard Quotient to Evaluate Pesticide Residues Detected in Pollen Trapped from Honey Bees (Apis mellifera) Analysis of pollen trapped from honey bees as they return to their hives provides a method of monitoring fluctuations in one route of pesticide exposure over location and time. We collected pollen from apiaries in five locations in Connecticut, including urban, rural, and mixed agricultural sites, for periods from two to five years.

Pollen was analyzed for pesticide residues using a standard extraction method widely used for pesticides (QuEChERS) and liquid chromatography/mass spectrometric analysis. Sixty pesticides or metabolites were detected. BioMed Research International Volume 2014 (2014), Determination of Mineral, Trace Element, and Pesticide Levels in Honey Samples. GREENPEACE - AVRIL 2014 - AN ANALYSIS OF PESTICIDE RESIDUES IN COMB POLLEN (BEEBREAD) AND TRAPPED POLLEN FROM HONEY BEES ( APIS.

MOLECULES - 2014 - Determination of Pesticide Residues in Honeybees using Modified QUEChERS Sample Work-Up and Liquid Chromatogr. ASEAN - Multiresidue determination of pesticides in honey samples by gas chromatography–mass spectrometry and application in env. IndaBook Example: Cats Protection, Dog federation, Cow Determination of Cypermethrin and Chlorpyrifos in ... Anil N.Mahindrakar et al/Int.J. ChemTech Res.2010,2(2) 909 local markets. AGRICULTURAL SCIENCE 29/10/12 The Potential for Using Ozone to Decrease Pesticide Residues in Honey Bee Comb.

AGRICULTURAL SCIENCE 29/10/12 The Potential for Using Ozone to Decrease Pesticide Residues in Honey Bee Comb – guatemalt

J. Agric. Food Chem., 2003, Assessment of Pesticide Residues in Honey Samples from Portugal and Spain. GOVERNMENT OF INDIA - HONEY RESIDUE MONITORING PLAN (RMP) FOR EXPORT TO EU - YEAR 2012-13. The ScientificWorld Journal Volume 2012, Antibiotic, Pesticide, andMicrobial Contaminants of Honey: Human Health Hazards. GEORGIA DEPARTMENT OF AGRICULTURE - 2006 - Présentation : Determination of Pesticide Residues in Honey by Modified QuEChERS Extr.

CENTRE DE RECHERCHES APICOLES DE BERNE - 2003 - Résidus de pesticides dans le miel et la cire d'abeilles provenant de Suisse. Chinese Journal of Chromatography Volume 24, Issue 5, September 2006, Determination of Multiple Pesticide Residues in Honey Usin. Abstract An analytical method was developed for the simultaneous determination of 23 pesticide residues in various commercial honeys. Meanwhile, the characteristic ions and fragmentation mechanism of three pesticides in the process of electron impact ionization mass spectrometry (EI/MS) were evaluated. After the optimization of different parameters such as the extraction solvent, pesticides were extracted from honey with ethyl acetate in an ultrasonic bath, cleaned up on a Florisil column by an elution of mixture of hexane and ethyl acetate (7/3, v/v), and analyzed by gas chromatography-electron impact ionization mass spectrometry (GC-EI/MS) in the selected ion-monitoring mode (SIM) with PCB103 as internal standard.

Recovery studies were performed at 50, 100 and 200 μg/kg fortification levels for each pesticide, and the recoveries ranged from 82% to 120% with relative standard deviations between 1.8% and 11.0% for different pesticides. Key Words. INTECH - OCT 2011 - Pesticide Residues in Bee Products. Food Control - Pesticide residues levels in honey from apiaries located of Northern Poland. Abstract Concentration levels of 30 pesticide residues were measured in honey samples collected from apiaries in northern part of Poland (Pomerania) using method based on the QuEChERS extraction followed by liquid chromatography–tandem mass spectrometry with electron spray ionization (LC–ESI–MS/MS). In 29% of the samples were found positive for at least some of the target compounds.

Concentration of bifenthrin, fenpyroximate, methidathion, spinosad, thiamethoxam, and triazophos exceeded maximum residue levels (MRL) in five samples (11%), the kind of the residues being correlated to agriculture practices in the region. The maximum values of these pesticides were 14.5, 16.3, 25.7, 20.6, 20.2 and 20.3 ng/g respectively. Profenofos was the most abundant at concentration ranged from <LOQ to 17.2 ng/g. Highlights. Swedish University of Agricultural Sciences (UPPSALA) - 2011 - Development of a method for determination of pesticide residues i.

Cire d'abeilles et résidus (notamment phytopharmaceutiques)